Benzyl Alcohol → 2-Benzyloxy-5-methanesulfonyl-benzoic acid

HRID 2251286Notes

Reaction equation

HRID 2251286 reaction equation
[CH3:1][S:2]([C:5]1[CH:14]=[C:9]([C:10]([O:12]C)=[O:11])[C:8]([OH:15])=[CH:7][CH:6]=1)(=[O:4])=[O:3].[CH2:16](O)[C:17]1[CH:22]=[CH:21][CH:20]=[CH:19][CH:18]=1>>[CH2:16]([O:15][C:8]1[CH:7]=[CH:6][C:5]([S:2]([CH3:1])(=[O:4])=[O:3])=[CH:14][C:9]=1[C:10]([OH:12])=[O:11])[C:17]1[CH:22]=[CH:21][CH:20]=[CH:19][CH:18]=1

Participants

3

Reactant 2

HCID 244Benzyl AlcoholHCID 235031632-Hydroxy-5-methylsulfonylbenzoic acid methyl ester

Product 1

HCID 688266832-Benzyloxy-5-methanesulfonyl-benzoic acid

Procedure

The title compound was prepared in analogy to example 2.10 from methyl 5-(methanesulfonyl)salicylate and benzylalcohol. MS (m/e): 305.3 (M−H, 100%)

Sources & evidence

ORD record
ord-cbb654bab8d54d858b8a612333bf7f2a
Source dataset
uspto-grants-2008_01
Patent number
US07319099B2

Reaction notes

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