HuagongsheHuagongshe Chemistry Print Report · For research reference only
o-Toluenesulfonyl chloride → HCID 10227346, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | o-Toluenesulfonyl chloride | HCID 8623 | — |
| Reactant | HCID 22272520 | HCID 22272520 | — |
| Product | HCID 10227346 | HCID 10227346 | — |
Reaction Steps
The compound was synthesized from N-{2-amino-5-(4-t-butyloxycarbonyl-1,4-diazepan-1-yl)- phenyl}methanesulfonamide and o-toluenesulfonylchloride (87 mg, 0.455 mmol) to give before Boc-deprotection 175 mg of a purple solid. M+1 439.2 Calcd 438.14.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07319097B2 |
| Source dataset | uspto-grants-2008_01 |
| ORD ID | ord-ae88bd8e079345669ebeedfb520384d8 |
| Source note | uspto-grants-2008_01 |