Ammonia → HCID 23329202, compound

HRID 225152Notes

Reaction equation

HRID 225152 reaction equation
[CH2:1]([CH:7]1[O:9][C:8]1([C:15]([O:17][CH2:18][CH3:19])=[O:16])[C:10](OCC)=[O:11])[CH2:2][CH2:3][CH2:4][CH2:5][CH3:6].[NH3:20]>C(O)C>[NH2:20][C:10]([C:8]1([C:15]([O:17][CH2:18][CH3:19])=[O:16])[CH:7]([CH2:1][CH2:2][CH2:3][CH2:4][CH2:5][CH3:6])[O:9]1)=[O:11]

Participants

4

Reactant 2

HCID 222AmmoniaHCID 12272042HCID 12272042, compound

Product 1

HCID 23329202HCID 23329202, compound

Reagents, catalysts & solvents 1

HCID 702EthanolSolvent

Procedure

A solution of 8.0 g of 2A in 10 ml of ethanol was saturated with ammonia (gas) and the mixture was allowed to stand for 2 days at room temperature. The precipitate that formed was collected and recrystallized from pentane to give 2, as white crystals, mp: 58°-60° C.

Workup

  1. customThe precipitate that formed
  2. customwas collected
  3. customrecrystallized from pentane
  4. customto give 2

Sources & evidence

ORD record
ord-435b13a32db74b5b8449d5fd6dbb9c5d
Source dataset
uspto-grants-1980_11
Patent number
US04235923

Reaction notes

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