HuagongsheHuagongshe Chemistry Print Report · For research reference only
5-Bromo-1-indanone → 1-methyl-5-(1-oxo-2,3-dihydro-1H-inden-5-yl)-1H-pyrrole-2-carbonitrile
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5-Bromo-1-indanone | HCID 520695 | — |
| Reactant | 1-Methylpyrrole-2-carbonitrile | HCID 2064111 | — |
| Product | 1-methyl-5-(1-oxo-2,3-dihydro-1H-inden-5-yl)-1H-pyrrole-2-carbonitrile | HCID 24987018 | — |
Reaction Steps
The title compound was prepared from 5-bromo-1-indanone and 1-methyl-2-cyanopyrrole according to the coupling procedure as described in example 1. MS (ESI) m/z 237; HRMS: calcd for C15H12N2O+H+, 237.1022; found (ESI, [M+H]+), 237.1003; Anal. Calcd for C15H12N2O: C, 76.25; H, 5.12; N, 11.86. Found: C, 75.99; H, 4.92; N, 11.80.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07319152B2 |
| Source dataset | uspto-grants-2008_01 |
| ORD ID | ord-50db46f81c9c4906b8de4e8456125267 |
| Source note | uspto-grants-2008_01 |