p-Bromopropiophenone → HCID 24987374, compound

HRID 2251647Notes

Reaction equation

HRID 2251647 reaction equation
Br[C:2]1[CH:7]=[CH:6][C:5]([C:8](=[O:11])[CH2:9][CH3:10])=[CH:4][CH:3]=1.[CH3:12][N:13]1[CH:17]=[CH:16][CH:15]=[C:14]1[C:18]#[N:19]>>[CH3:12][N:13]1[C:17]([C:2]2[CH:7]=[CH:6][C:5]([C:8](=[O:11])[CH2:9][CH3:10])=[CH:4][CH:3]=2)=[CH:16][CH:15]=[C:14]1[C:18]#[N:19]

Participants

3

Reactant 2

HCID 66312p-BromopropiophenoneHCID 20641111-Methylpyrrole-2-carbonitrile

Product 1

HCID 24987374HCID 24987374, compound

Procedure

The title compound was prepared from 1-(4-bromophenyl)-propan-1-one and 1-methyl-2-cyanopyrrole according to the coupling procedure as described in example 1. MS (ES) m/z 239.2; HRMS: calcd for C15H14N2O+H+, 239.1179; found (ESI, [M+H]+), 239.1193.

Sources & evidence

ORD record
ord-4d6b45584d8c47c8b893044169b07ff2
Source dataset
uspto-grants-2008_01
Patent number
US07319152B2

Reaction notes

Loading…