Hexylamine → HCID 23329160, compound

HRID 225165Notes

Reaction equation

HRID 225165 reaction equation
[Cl:1][C:2]1[CH:7]=[CH:6][C:5]([C:8](=[O:14])[CH2:9][CH2:10][C:11](O)=[O:12])=[CH:4][C:3]=1[S:15](=[O:24])(=[O:23])[NH:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH3:22].[CH2:25]([NH2:31])CCCCC>>[Cl:1][C:2]1[CH:7]=[CH:6][C:5]([C:8]2([OH:14])[N:31]([CH3:25])[C:11](=[O:12])[CH2:10][CH2:9]2)=[CH:4][C:3]=1[S:15](=[O:24])(=[O:23])[NH:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH3:22]

Participants

3

Reactant 2

HCID 8102HexylamineHCID 23329093HCID 23329093, compound

Product 1

HCID 23329160HCID 23329160, compound

Procedure

The 4-(4-chloro-3-n-hexylsulfamoylphenyl)-4-oxobutanoic acid required is obtained analogously to the instructions indicated in Example 15(a) using 7.5 g of n-hexylamine.

Sources & evidence

ORD record
ord-b18c330d91bf4c41b6bdf4ba91813545
Source dataset
uspto-grants-1980_11
Patent number
US04235918

Reaction notes

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