(3-Methoxyphenyl)boronic acid → HCID 57786916, compound
Reaction equation
[O:1]=[C:2]1[CH2:11][CH2:10][CH2:9][C:8]2[CH:7]=[C:6](OS(C(F)(F)F)(=O)=O)[CH:5]=[CH:4][C:3]1=2.[CH3:20][O:21][C:22]1[CH:23]=[C:24](B(O)O)[CH:25]=[CH:26][CH:27]=1>>[CH3:20][O:21][C:22]1[CH:27]=[C:26]([C:6]2[CH:7]=[C:8]3[C:3](=[CH:4][CH:5]=2)[C:2](=[O:1])[CH2:11][CH2:10][CH2:9]3)[CH:25]=[CH:24][CH:23]=1Participants
3
Procedure
The title compound was prepared from trifluoro-methanesulfonic acid 5-oxo-5,6,7,8-tetrahydro-naphthalen-2-yl ester and 3-methoxyphenyl boronic acid according to the coupling procedure as described in example 6. MS (ESI) m/z 253.
Sources & evidence
- ORD record
- ord-7a6415d5ee534c22ae44f2ac801b2cd3
- Source dataset
- uspto-grants-2008_01
- Patent number
- US07319152B2
Reaction notes
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