(3-Chlorophenyl)boronic acid → HCID 45483812, compound

HRID 2251667Notes

Reaction equation

HRID 2251667 reaction equation
[CH3:1][C:2]1([CH3:20])[C:10]2[C:5](=[CH:6][CH:7]=[C:8](OS(C(F)(F)F)(=O)=O)[CH:9]=2)[C:4](=[O:19])[CH2:3]1.[Cl:21][C:22]1[CH:23]=[C:24](B(O)O)[CH:25]=[CH:26][CH:27]=1>>[Cl:21][C:22]1[CH:27]=[C:26]([C:8]2[CH:9]=[C:10]3[C:5](=[CH:6][CH:7]=2)[C:4](=[O:19])[CH2:3][C:2]3([CH3:20])[CH3:1])[CH:25]=[CH:24][CH:23]=1

Participants

3

Reactant 2

HCID 2734323(3-Chlorophenyl)boronic acidHCID 57618520Trifluoromethanesulfonic acid 3,3-dimethyl-1-oxo-indan-5-yl ester

Product 1

HCID 45483812HCID 45483812, compound

Procedure

The title compound was prepared from trifluoro-methanesulfonic acid 3,3-dimethyl-1-oxo-indan-5-yl ester and 3-chlorophenyl boronic acid according to the procedure described in example 21. MS (ES) m/z 271.1; HRMS: calcd for C17H15ClO+H+, 271.08842; found (ESI, [M+H]+), 271.0881.

Sources & evidence

ORD record
ord-e81390cc49ad4cc4900897f5f1bd8a6a
Source dataset
uspto-grants-2008_01
Patent number
US07319152B2

Reaction notes

Loading…