3-Tolylboronic acid → HCID 45483822, compound

HRID 2251668Notes

Reaction equation

HRID 2251668 reaction equation
[CH3:1][C:2]1([CH3:20])[C:10]2[C:5](=[CH:6][CH:7]=[C:8](OS(C(F)(F)F)(=O)=O)[CH:9]=2)[C:4](=[O:19])[CH2:3]1.[CH3:21][C:22]1[CH:23]=[C:24](B(O)O)[CH:25]=[CH:26][CH:27]=1>>[CH3:1][C:2]1([CH3:20])[C:10]2[C:5](=[CH:6][CH:7]=[C:8]([C:26]3[CH:25]=[CH:24][CH:23]=[C:22]([CH3:21])[CH:27]=3)[CH:9]=2)[C:4](=[O:19])[CH2:3]1

Participants

3

Reactant 2

HCID 27339503-Tolylboronic acidHCID 57618520Trifluoromethanesulfonic acid 3,3-dimethyl-1-oxo-indan-5-yl ester

Product 1

HCID 45483822HCID 45483822, compound

Procedure

The title compound was prepared from trifluoro-methanesulfonic acid 3,3-dimethyl-1-oxo-indan-5-yl ester and 3-methylphenyl boronic acid according to the procedure described in example 21. MS (ES) m/z 251.2; HRMS: calcd for C18H18O+H+, 251.14304; found (ESI, [M+H]+), 251.1428.

Sources & evidence

ORD record
ord-96a63d9619d94b53b1b1461d5e874ff4
Source dataset
uspto-grants-2008_01
Patent number
US07319152B2

Reaction notes

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