(3-Methoxyphenyl)boronic acid → HCID 69037106, compound

HRID 2251669Notes

Reaction equation

HRID 2251669 reaction equation
[CH3:1][C:2]1([CH3:20])[C:10]2[C:5](=[CH:6][CH:7]=[C:8](OS(C(F)(F)F)(=O)=O)[CH:9]=2)[C:4](=[O:19])[CH2:3]1.[CH3:21][O:22][C:23]1[CH:24]=[C:25](B(O)O)[CH:26]=[CH:27][CH:28]=1>>[CH3:21][O:22][C:23]1[CH:28]=[C:27]([C:8]2[CH:9]=[C:10]3[C:5](=[CH:6][CH:7]=2)[C:4](=[O:19])[CH2:3][C:2]3([CH3:20])[CH3:1])[CH:26]=[CH:25][CH:24]=1

Participants

3

Reactant 2

HCID 2734370(3-Methoxyphenyl)boronic acidHCID 57618520Trifluoromethanesulfonic acid 3,3-dimethyl-1-oxo-indan-5-yl ester

Product 1

HCID 69037106HCID 69037106, compound

Procedure

The title compound was prepared from trifluoro-methanesulfonic acid 3,3-dimethyl-1-oxo-indan-5-yl ester and 3-methoxyphenyl boronic acid according to the procedure described in example 21. MS (ES) m/z 267.2; HRMS: calcd for C18H18O2+H+, 267.13796; found (ESI, [M+H]+), 267.1386.

Sources & evidence

ORD record
ord-95c36f69341d4ee3935316e7a062ebce
Source dataset
uspto-grants-2008_01
Patent number
US07319152B2

Reaction notes

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