HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-(Dimethylamino)phenylboronic acid → 5-[4-(Dimethylamino)phenyl]-3,3-dimethylindan-1-one
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-(Dimethylamino)phenylboronic acid | HCID 2734344 | — |
| Reactant | Trifluoromethanesulfonic acid 3,3-dimethyl-1-oxo-indan-5-yl ester | HCID 57618520 | — |
| Product | 5-[4-(Dimethylamino)phenyl]-3,3-dimethylindan-1-one | HCID 69036611 | — |
Reaction Steps
The title compound was prepared from trifluoro-methanesulfonic acid 3,3-dimethyl-1-oxo-indan-5-yl ester and 4-(dimethylamino)phenyl boronic acid according to the procedure described in example 21. MS m/z 280; HRMS: calcd for C19H21NO+H+, 280.16959; found (ESI, [M+H]+), 280.1691.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07319152B2 |
| Source dataset | uspto-grants-2008_01 |
| ORD ID | ord-4ec41c1e185644869a6bcac665ee4415 |
| Source note | uspto-grants-2008_01 |