3-(Dimethylamino)benzeneboronic acid → HCID 69035359, compound

HRID 2251681Notes

Reaction equation

HRID 2251681 reaction equation
[CH3:1][C:2]1([CH3:20])[C:10]2[C:5](=[CH:6][CH:7]=[C:8](OS(C(F)(F)F)(=O)=O)[CH:9]=2)[C:4](=[O:19])[CH2:3]1.[CH3:21][N:22]([CH3:32])[C:23]1[CH:24]=[C:25](B(O)O)[CH:26]=[CH:27][CH:28]=1>>[CH3:21][N:22]([CH3:32])[C:23]1[CH:28]=[C:27]([C:8]2[CH:9]=[C:10]3[C:5](=[CH:6][CH:7]=2)[C:4](=[O:19])[CH2:3][C:2]3([CH3:20])[CH3:1])[CH:26]=[CH:25][CH:24]=1

Participants

3

Reactant 2

HCID 27625273-(Dimethylamino)benzeneboronic acidHCID 57618520Trifluoromethanesulfonic acid 3,3-dimethyl-1-oxo-indan-5-yl ester

Product 1

HCID 69035359HCID 69035359, compound

Procedure

The title compound was prepared from trifluoro-methanesulfonic acid 3,3-dimethyl-1-oxo-indan-5-yl ester and 3-(dimethylamino)phenyl boronic acid according to the procedure described in example 21. MS m/z 280; HRMS: calcd for C19H21NO+H+, 280.16959; found (ESI, [M+H]+), 280.1689.

Sources & evidence

ORD record
ord-d7a0af252ae44e3e9c803e76aa4bcf40
Source dataset
uspto-grants-2008_01
Patent number
US07319152B2

Reaction notes

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