3-Acetylphenylboronic acid → HCID 69039120, compound

HRID 2251686Notes

Reaction equation

HRID 2251686 reaction equation
[CH3:1][C:2]1([CH3:20])[C:10]2[C:5](=[CH:6][CH:7]=[C:8](OS(C(F)(F)F)(=O)=O)[CH:9]=2)[C:4](=[O:19])[CH2:3]1.[C:21]([C:24]1[CH:25]=[C:26](B(O)O)[CH:27]=[CH:28][CH:29]=1)(=[O:23])[CH3:22]>>[C:21]([C:24]1[CH:29]=[C:28]([C:8]2[CH:9]=[C:10]3[C:5](=[CH:6][CH:7]=2)[C:4](=[O:19])[CH2:3][C:2]3([CH3:20])[CH3:1])[CH:27]=[CH:26][CH:25]=1)(=[O:23])[CH3:22]

Participants

3

Reactant 2

HCID 27343103-Acetylphenylboronic acidHCID 57618520Trifluoromethanesulfonic acid 3,3-dimethyl-1-oxo-indan-5-yl ester

Product 1

HCID 69039120HCID 69039120, compound

Procedure

The title compound was prepared from trifluoro-methanesulfonic acid 3,3-dimethyl-1-oxo-indan-5-yl ester and 3-acetyl phenyl boronic acid according to the procedure described in example 21. MS (ESI) m/z 279; HRMS: calcd for C19H18O2+H+, 279.13796; found (ESI, [M+H]+), 279.1374.

Sources & evidence

ORD record
ord-349bbdac7f18432888b2b61ac8a9eb97
Source dataset
uspto-grants-2008_01
Patent number
US07319152B2

Reaction notes

Loading…