HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Acetylphenylboronic acid → 5-(2-Acetylphenyl)-3,3-dimethylindan-1-one
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Acetylphenylboronic acid | HCID 2734309 | — |
| Reactant | Trifluoromethanesulfonic acid 3,3-dimethyl-1-oxo-indan-5-yl ester | HCID 57618520 | — |
| Product | 5-(2-Acetylphenyl)-3,3-dimethylindan-1-one | HCID 69035890 | — |
Reaction Steps
The title compound was prepared from trifluoro-methanesulfonic acid 3,3-dimethyl-1-oxo-indan-5-yl ester and 2-acetylphenyl boronic acid according to the procedure described in example 21. MS (ESI) m/z 279; HRMS: calcd for C19H18O2+H+, 279.13796; found (ESI, [M+H]+), 279.1383.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07319152B2 |
| Source dataset | uspto-grants-2008_01 |
| ORD ID | ord-1126abde05a344ecbc4b33aeffa8b17b |
| Source note | uspto-grants-2008_01 |