HuagongsheHuagongshe Chemistry Print Report · For research reference only
Oxalyl chloride → HCID 86592611, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Oxalyl chloride | HCID 65578 | — |
| Reactant | HCID 68614820 | HCID 68614820 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 86592611 | HCID 86592611 | — |
Reaction Steps
Part B: To a stirred solution of 1-(chlorophenyl)-5-(2,4-dichlorophenyl)-1H-1,2,4-triazole-3-carboxylic acid (0.37 g, 1.00 mmol) in dichloromethane (10 mL) is added oxalyl chloride (0.254 g, 2.00 mmol). The resulting mixture is concentrated in vacuo to give crude 1-(chlorophenyl)-5-(2,4-dichlorophenyl)-1H-1,2,4-triazole-3-carbonyl chloride.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07319110B2 |
| Source dataset | uspto-grants-2008_01 |
| ORD ID | ord-9d13a8f2d9f9473db3be7f077facc725 |
| Source note | uspto-grants-2008_01 |