HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Nitrobenzenesulfonamide → HCID 10211643, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Nitrobenzenesulfonamide | HCID 22784 | — |
| Reactant | HCID 22242280 | HCID 22242280 | — |
| Product | HCID 10211643 | HCID 10211643 | 69% |
Reaction Steps
3,5-Dibromo-4-(3-bromobenzyloxy)benzoic acid (0.13 mmol) was coupled with 4-nitrobenzenesulphonamide (0.64 mmol) using the procedure described in Example 31. Purification on column (silica gel, chloroform/methanol 9:1) gave 58 mg (69%) of N-[3,5-dibromo-4-(3-bromobenzyloxy)benzoyl]-4-nitrobenzene-sulphonamide.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07319163B2 |
| Source dataset | uspto-grants-2008_01 |
| ORD ID | ord-de7ae4cd0886471e8639e9c66e1006bc |
| Source note | uspto-grants-2008_01 |