Dimethylcarbamoyl Chloride → HCID 15586944, compound

Participants

Reaction Steps

The process is carried out as in Example 4 with the difference that 0.6 g (0.00213 moles) of 6-methyl-8β-hydrazinomethyl-ergoline and 0.25 g (0.00234 moles) of dimethylcarbamoyl chloride are used as the starting substances. 0.5 g (69%) of 6-methyl-8β-([N'-dimethylcarbamoyl-hydrazino]-methyl)-ergoline are obtained; m.p.: 205°-206° C., [α]D20 =-36.2° (c=1, in 96% ethanol).

Provenance & Evidence