HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 225204Generated: October 31, 2026
Dimethyl itaconate → HCID 53909143, compound
https://huagongshe.com/reaction/225204
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Dimethyl itaconate | HCID 69240 | — |
| Reactant | Sodium Methoxide | HCID 10942334 | — |
| Reactant | Dimethylphosphite | HCID 21884954 | — |
| Product | HCID 53909143 | HCID 53909143 | — |
Reaction Steps
8 ml of a 30% sodium methylate solution are added dropwise to 158 g (1 mol) of itaconic acid dimethyl ester and 110 g of dimethyl phosphite at 60° C. The exothermic reaction is by that time completed. The mixture is then stirred for one hour at 100° C. and concentrated by evaporation. Quantitative yield of a colorless liquid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US04235976 |
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| Source dataset | uspto-grants-1980_11 |
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| ORD ID | ord-0fad8bd770134a5ab62dc39be89d6f84 |
|---|
| Source note | uspto-grants-1980_11 |
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