Ammonia → HCID 9995256, compound

Participants

Reaction Steps

The desired product was prepared by replacing Example 1C and 4-carboxybenzene boronic acid with Example 19A and 4-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)-benzamide in Example 1D. MS (DCI/NH3) m/z: 306.1 (M+H)+; 1H NMR (500 MHz, DMSO-d6) δ 3.90 (s, 2H), 4.57 (s, 2H), 7.32 (d, J=7.49 Hz, 1H), 7.54 (s, 1H), 7.61 (d, J=7.80 Hz, 1H), 7.89 (d, J=8.42 Hz, 2H), 8.00 (d, J=8.42 Hz, 2H).

Provenance & Evidence