Ammonia → HCID 10267080, compound

Participants

Reaction Steps

The desired product was prepared by replacing Example 1C and 4-carboxybenzene boronic acid with Example 44C and 4-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)-benzamide in Example 1D. MS (DCI/NH3) m/z: 306.0 (M+H)+; 1H NMR (500 MHz, DMSO-d6) δ 3.88 (s, 2H), 4.59 (s, 2H), 5.22 (s, 1H), 7.25 (d, J=7.80 Hz, 1H), 7.32-7.45 (m, 1H), 7.52 (d, J=7.80 Hz, 1H), 7.65 (s, 1H), 7.88 (s, 2H), 7.99 (d, J=7.80 Hz, 2H), 13.29 (s, 1H).

Provenance & Evidence