HuagongsheHuagongshe Chemistry Print Report · For research reference only
tert-Butyl piperazine-1-carboxylate → tert-Butyl 4-[5-chloro-1-(4-chlorophenyl)-6-oxo-1,6-dihydro-4-pyridazinyl]-1-piperazine carboxylate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | tert-Butyl piperazine-1-carboxylate | HCID 143452 | — |
| Reactant | 4,5-Dichloro-2-(4-chlorophenyl)-3(2H)-pyridazinone | HCID 779402 | — |
| Product | tert-Butyl 4-[5-chloro-1-(4-chlorophenyl)-6-oxo-1,6-dihydro-4-pyridazinyl]-1-piperazine carboxylate | HCID 58585184 | — |
Reaction Steps
By general method 1 from 20.66 g (75 mmol) of 2-(4-chlorophenyl)-4,5-dichloropyridazin-3-one with 25.14 g (135 mmol) of Boc-piperazine.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07320977B2 |
| Source dataset | uspto-grants-2008_01 |
| ORD ID | ord-bd1cf704a1e743c0bfabb7300c9d38c0 |
| Source note | uspto-grants-2008_01 |