Methanesulfonyl chloride → HCID 58585193, compound

HRID 2252282Notes

Reaction equation

HRID 2252282 reaction equation
[Cl:1][C:2]1[C:3](=[O:21])[N:4]([C:14]2[CH:19]=[CH:18][C:17]([Cl:20])=[CH:16][CH:15]=2)[N:5]=[CH:6][C:7]=1[N:8]1[CH2:13][CH2:12][NH:11][CH2:10][CH2:9]1.[CH3:22][S:23](Cl)(=[O:25])=[O:24]>>[Cl:1][C:2]1[C:3](=[O:21])[N:4]([C:14]2[CH:15]=[CH:16][C:17]([Cl:20])=[CH:18][CH:19]=2)[N:5]=[CH:6][C:7]=1[N:8]1[CH2:9][CH2:10][N:11]([S:23]([CH3:22])(=[O:25])=[O:24])[CH2:12][CH2:13]1

Participants

3

Reactant 2

HCID 31297Methanesulfonyl chlorideHCID 58585369HCID 58585369, compound

Product 1

HCID 58585193HCID 58585193, compound

Procedure

Obtainable by general method 4 from 10.0 g (30.75 mmol) of the compound from Example 2A with 3.6 ml (46.1 mmol) of methanesulfonyl chloride.

Sources & evidence

ORD record
ord-478fcf0cec5c44b98291595fbc82323c
Source dataset
uspto-grants-2008_01
Patent number
US07320977B2

Reaction notes

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