Sodium Azide → HCID 58585370, compound

HRID 2252283Notes

Reaction equation

[C:1]1([C:23]2[CH:28]=[CH:27][CH:26]=[CH:25][CH:24]=2)[CH:6]=[CH:5][C:4]([O:7][C:8]2[C:9](=[O:22])[N:10]([C:15]3[CH:20]=[CH:19][C:18]([Cl:21])=[CH:17][CH:16]=3)[N:11]=[CH:12][C:13]=2Cl)=[CH:3][CH:2]=1.[N-:29]=[N+:30]=[N-:31].[Na+]>>[N:29]([C:13]1[CH:12]=[N:11][N:10]([C:15]2[CH:20]=[CH:19][C:18]([Cl:21])=[CH:17][CH:16]=2)[C:9](=[O:22])[C:8]=1[O:7][C:4]1[CH:5]=[CH:6][C:1]([C:23]2[CH:28]=[CH:27][CH:26]=[CH:25][CH:24]=2)=[CH:2][CH:3]=1)=[N+:30]=[N-:31]

Participants

Reactant 2

HCID 33557Sodium Azide

HCID 58585361HCID 58585361, compound

Product 1

HCID 58585370HCID 58585370, compound

Procedure

Obtainable by general method 13 from 2.05 g (5.0 mmol) of the compound from Example 9A with 1.63 g (25.0 mmol) of sodium azide.

Sources & evidence

ORD record: ord-2b1f1b43b1724d7da8e12263557629e1
Source dataset: uspto-grants-2008_01
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US07320977B2

Reaction notes

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