Sodium Azide → HCID 58585208, compound

HRID 2252284Notes

Reaction equation

HRID 2252284 reaction equation
[Br:1][C:2]1[CH:23]=[CH:22][C:5]([O:6][C:7]2[C:8](=[O:21])[N:9]([C:14]3[CH:19]=[CH:18][C:17]([Cl:20])=[CH:16][CH:15]=3)[N:10]=[CH:11][C:12]=2Cl)=[CH:4][CH:3]=1.[N-:24]=[N+:25]=[N-:26].[Na+]>>[N:24]([C:12]1[CH:11]=[N:10][N:9]([C:14]2[CH:19]=[CH:18][C:17]([Cl:20])=[CH:16][CH:15]=2)[C:8](=[O:21])[C:7]=1[O:6][C:5]1[CH:22]=[CH:23][C:2]([Br:1])=[CH:3][CH:4]=1)=[N+:25]=[N-:26]

Participants

3

Procedure

Obtainable by general method 13 from 7.55 g (18.3 mmol) of the compound from Example 10A with 5.96 g (91.6 mmol) of sodium azide.

Sources & evidence

ORD record
ord-23ab36d072b7444bbf3920cb514179f5
Source dataset
uspto-grants-2008_01
Patent number
US07320977B2

Reaction notes

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