Dichloromethane → HCID 58585338, compound

Participants

Reaction Steps

0.2 g (0.424 mmol) of the compound from Example 14 are dissolved in 7 ml of methanol and, at room temperature, 50 mg (1.3 mmol) of sodium borohydride are added in portions. Stirring for 2 h is followed by dilution with dichloromethane, washing with saturated ammonium chloride solution, drying over sodium sulfate and concentration. The crude product is stirred with 25 ml of boiling methanol and then cooled and filtered off with suction.

Provenance & Evidence