HRID225232

反应详情

EQUATION

反应方程式

HRID 225232 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

A mixture of 3.15 g. of 3-dimethylamino-3'-(trifluoromethyl)acrylophenone and 1.40 g. of 3-aminopyrazole-4-carbonitrile in 25 ml. of glacial acetic acid is refluxed for 6 hours. The mixture is evaporated and the residue is treated as described in Example 1, giving the desired product, m.p. 144°-145° C.

WORKUP

后处理

  1. additionA mixture of 3.15 g
  2. customThe mixture is evaporated
  3. additionthe residue is treated