HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Methoxybenzaldehyde → HCID 69099875, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Methoxybenzaldehyde | HCID 31244 | — |
| Reactant | Diethyl (4-isopropyl-3,5-dimethoxybenzyl)phosphonate | HCID 46928247 | — |
| Product | HCID 69099875 | HCID 69099875 | 63% |
Reaction Steps
This material was prepared from diethyl(3,5-dimethoxy-4-i-propylbenzyl)phosphonate and 4-anisaldehyde in 63% yield as the same procedure as described in example 5(b). 1H NMR (CDCl3, ppm): δ 1.31 (d, J=7.1 Hz, 6H), 3.51-3.74 (m, 1H), 3.86 (s, 3H), 3.91 (s, 6H), 6.71 (s, 2H), 6.84-7.09 (m, 4H), 7.39-7.60 (m, 2H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07321050B2 |
| Source dataset | uspto-grants-2008_01 |
| ORD ID | ord-83dcbe07283348e192cebb06eb0cabd8 |
| Source note | uspto-grants-2008_01 |