HuagongsheHuagongshe Chemistry Print Report · For research reference only
Pyridinium chloride → 5-[2-(4-Hydroxyphenyl)ethenyl]-2-i-propyl-1,3-benzenediol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Pyridinium chloride | HCID 10176127 | — |
| Reactant | HCID 69099875 | HCID 69099875 | — |
| Product | 5-[2-(4-Hydroxyphenyl)ethenyl]-2-i-propyl-1,3-benzenediol | HCID 66842847 | 30% |
Reaction Steps
This material was prepared from 1-(3,5-dimethoxy-4-i-propylphenyl)-2-(4-methoxyphenyl)ethene and pyridine hydrochloride in 30% yield in the same way as described in example 3. 1H NMR (DMSO-d6, ppm): δ 1.22 (d, J=7.0 Hz, 6H), 3.41 (m, 1H), 6.40 (s, 2H), 6.73 (d, J=6.3 Hz, 4H), 7.33 (s, 1H), 7.41 (s, 1H), 8.98 (s, 2H), 9.51 (s, 1H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07321050B2 |
| Source dataset | uspto-grants-2008_01 |
| ORD ID | ord-375652e2d1374a46af931a5d0c0ea16f |
| Source note | uspto-grants-2008_01 |