HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-(2-Amino-5-bromophenyl)ethan-1-one → 1-(2-Amino-5-bromophenyl)-1-phenylethanol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-(2-Amino-5-bromophenyl)ethan-1-one | HCID 11074746 | — |
| Reactant | HCID 178418255 | HCID 178418255 | — |
| Product | 1-(2-Amino-5-bromophenyl)-1-phenylethanol | HCID 68865054 | — |
Reaction Steps
Prepared from 1-(2-amino-5-bromo-phenyl)-ethanone and phenyl magnesium bromide generally according to the procedure described in example 1. 1H-NMR (DMSO-d6) δ 7.32-7.16 (m, 6H), 7.11 (dd, J=2.03, 8.48 Hz, 1H), 6.49 (d, J=8.55 Hz, 1H), 6.02 (s, 1H), 5.16 (s, 2H), 1.74 (s, 3H); MS (ES) m/z 274/276 ([M+H]+, 100%); Anal. Calc. For C14H14BrNO: C: 57.55; H: 4.83; N: 4.79. Found: C: 57.67; H: 4.83; N: 4.79.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07323455B2 |
| Source dataset | uspto-grants-2008_01 |
| ORD ID | ord-5b2ec3ac8d7b4b67a235543383e31c9b |
| Source note | uspto-grants-2008_01 |