Methyl 2-amino-5-bromobenzoate → HCID 68864279, compound

Participants

Reaction Steps

Prepared from methyl 2-amino-5-bromobenzoate and 3-furyllithium following the procedure described in example 24. 1H NMR (DMSO-d6): δ 7.6 (t, J=1.73 Hz, 2H), 7.25 (q, J=1.51, 0.81 Hz, 2H), 7.10 (q, J=8.46, 2.43 Hz, 1H), 6.79 (d, J=2.43 Hz, 1H), 6.56 (d, J=8.46 Hz, 1H), 6.46 (d, J=8.46 Hz, 1H), 6.39 (q, J=1.73, 0.81 Hz, 2H), 5.35 (s, 2H); MS (ESI) m/z 332/334 ([M−H]−).

Provenance & Evidence