HRID2252615

反应详情

EQUATION

反应方程式

HRID 2252615 的结构方程式

PROCEDURE

实验过程

This compound was obtained in 97% yield according to the procedure described in the synthesis of N-tert-butyl-(1-methyl)cyclopropylsulfonamide except 1.25 equivalents of allyl bromide were used as electrophile. The compound was taken directly into the next reaction without purification: 1H NMR (CDCl3) δ 0.83 (m, 2H), 1.34 (s, 9H), 1.37 (m, 2H), 2.64 (d, J=7.3 Hz, 2H), 4.25 (br s, 1H), 5.07-5.10 (m, 2H), 6.70-6.85 (m, 1H).

WORKUP

后处理

  1. customThis compound was obtained in 97% yield
  2. customThe compound was taken directly into the next reaction without purification