HuagongsheHuagongshe Chemistry Print Report · For research reference only
p-Toluenesulfonic acid → HCID 10173124, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | p-Toluenesulfonic acid | HCID 6101 | — |
| Reactant | 3-Aminobenzonitrile | HCID 16702 | — |
| Reactant | HCID 10126479 | HCID 10126479 | — |
| Product | HCID 10173124 | HCID 10173124 | 57% |
Reaction Steps
Intermediate 6, (0.10 g, 0.30 mmol) and 3-cyanoaniline (0.05 g, 0.45 mmol) were reacted together following the procedure detailed for the compound of Example 2, with the addition of an equivalent of tosic acid which eventually gave the title compound as a white solid (0.07 g, 57%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07323464B2 |
| Source dataset | uspto-grants-2008_01 |
| ORD ID | ord-8d0e5708c8874a1b81a5c9ef9346441e |
| Source note | uspto-grants-2008_01 |