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HRID225277

反应详情

EQUATION

反应方程式

HRID 225277 的结构方程式

REACTANTS

反应物

2
结构：CN(C)C=CC(=O)c1cccc(C(F)(F)F)c1
HCID730024

未命名化合物

结构：CCOC(=O)c1nc[nH]c1N
HCID178470302

未命名化合物

PRODUCTS

生成物

1
结构：CCOC(=O)c1ncn2c(-c3cccc(C(F)(F)F)c3)ccnc12
HCID23329853

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CC(=O)O
溶剂HCID176

Acetic Acid

C2H4O2

PROCEDURE

实验过程

A mixture of 1.55 g. of ethyl 5-aminoimidazole-4-carboxylate and 2.43 g. of 3-dimethylamino-3'-trifluoromethylacrylophenone in 25 ml. of glacial acetic acid is refluxed for 6 hours. On cooling the product crystallized from solution, m.p. 232°-234° C.

WORKUP

后处理

  1. additionA mixture of 1.55 g
  2. temperatureOn cooling the product
  3. customcrystallized from solution, m.p. 232°-234° C.