HuagongsheHuagongshe Chemistry Print Report · For research reference only
3,4-Dimethoxyphenyl methyl ketone → (E)-1-(3,4-dimethoxyphenyl)-3-(dimethylamino)-2-propen-1-one
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3,4-Dimethoxyphenyl methyl ketone | HCID 14328 | — |
| Reactant | Dimethylformamide dimethyl acetal | HCID 78373 | — |
| Product | (E)-1-(3,4-dimethoxyphenyl)-3-(dimethylamino)-2-propen-1-one | HCID 1481361 | — |
Reaction Steps
A mixture of 50.0 g. of 3',4'-dimethoxyacetophenone and 50 ml. of dimethylformamide dimethylacetal is refluxed for 16 hours. On cooling the desired compound crystallizes from solution. Hexane is added and the material is recovered by filtration, m.p. 124°-125° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04236005 |
| Source dataset | uspto-grants-1980_11 |
| ORD ID | ord-54c4480f822a4aa3a9d351bb9039ec04 |
| Source note | uspto-grants-1980_11 |