HRID225282

反应详情

EQUATION

反应方程式

HRID 225282 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

A mixture of 4.07 g. of 3-dimethylamino-4'-ethylacrylophenone and 3.10 g. of ethyl 3-aminopyrazole-4-carboxylate in 25 ml. of glacial acetic acid is refluxed for 20 hours. The compound is recovered from the reaction in the previously described fashion to yield crystals, m.p. 101°-103° C.

WORKUP

后处理

  1. additionA mixture of 4.07 g
  2. customThe compound is recovered from the reaction in the previously described fashion
  3. customto yield crystals, m.p. 101°-103° C.