HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Fluorophenylboronic acid → HCID 59639523, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Fluorophenylboronic acid | HCID 2734354 | — |
| Reactant | HCID 9944656 | HCID 9944656 | — |
| Product | HCID 59639523 | HCID 59639523 | — |
Reaction Steps
Prepared as described above in Example 11 starting from 4-chloro-6-(2-chloro-phenylamino)-2-methylsulfanyl-pyrimidine-5-carbaldehyde and 2-fluorophenylboronic acid to give the title compound 4-(2-fluoro-phenyl)-6-(2-chloro-phenylanmino)-2-methylsulfanyl-pyrimidine-5-carbaldehyde. 1H-NMR: δ 2.60 (s, 3H), 6.99-7.68 (m, 7H), 8.47 (d, 1H, J=4.7 Hz), 9.78 (s, 1H), 11.59 (br s, 1H). LC MS (m/e)=374 (MH+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07323472B2 |
| Source dataset | uspto-grants-2008_01 |
| ORD ID | ord-190c96c4b76d40d1b1e4715b35b13a77 |
| Source note | uspto-grants-2008_01 |