HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → CID 3084433
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | Toluene | HCID 1140 | — |
| Product | CID 3084433 | HCID 3084433 | — |
Reaction Steps
200 ml of an acidic ion-exchange resin (Bio-Rad 50W-X2) was added to the mixture and it was stirred for 1.5 hours. 200 ml of toluene was added to the mixture and water was removed by azeotropic distillation. The product was filtered to remove the resin, and the solvent was removed under reduced pressure. The resulting diol (482 g) had a hydroxyl number of 67 mg KOH/g.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04236020 |
| Source dataset | uspto-grants-1980_11 |
| ORD ID | ord-2e87ed9e326d45a99ce4bd51c5c78e56 |
| Source note | uspto-grants-1980_11 |