Glycine → HCID 66713069, compound

HRID 2253147Notes

Reaction equation

[CH3:1][C:2]1[CH:20]=[CH:19][CH:18]=[C:17]([CH3:21])[C:3]=1[O:4][C:5]1[CH:6]=[C:7]([C:14]([OH:16])=O)[C:8](=[CH:12][CH:13]=1)[C:9]([OH:11])=O.[NH2:22][CH2:23][C:24]([OH:26])=[O:25].[CH3:27]O>>[CH3:27][O:25][C:24](=[O:26])[CH2:23][N:22]1[C:14](=[O:16])[C:7]2[C:8](=[CH:12][CH:13]=[C:5]([O:4][C:3]3[C:17]([CH3:21])=[CH:18][CH:19]=[CH:20][C:2]=3[CH3:1])[CH:6]=2)[C:9]1=[O:11]

Participants

Reactant 3

HCID 750Glycine

HCID 887Methanol

HCID 17846255HCID 17846255, compound

Product 1

HCID 66713069HCID 66713069, compound

Procedure

4-(2,6-dimethyl-phenoxy)-phthalic acid was reacted with glycine in analogy to Example D-1 b). The crude product was then reacted with methanol in analogy to Example D-1 c); 1H NMR (CDCl3): δ=7.80 (d, 1H), 7.09 to 7.17 (m, 5H), 4.40 (s, 2H), 3.76 (s, 3H), 2.11 (s, 6H).

Sources & evidence

ORD record: ord-6f02c021621a44d89b4ee69f2b8f1972
Source dataset: uspto-grants-2008_01
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US07323475B2

Reaction notes

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