Sodium Azide → HCID 23329761, compound

HRID 225317Notes

Reaction equation

HRID 225317 reaction equation
Cl[CH2:2][C:3]1[CH:4]=[C:5]([CH2:10][C:11]([OH:13])=[O:12])[CH:6]=[CH:7][C:8]=1[OH:9].[N-:14]=[N+:15]=[N-:16].[Na+]>O>[N:14]([CH2:2][C:3]1[CH:4]=[C:5]([CH2:10][C:11]([OH:13])=[O:12])[CH:6]=[CH:7][C:8]=1[OH:9])=[N+:15]=[N-:16]

Participants

4

Reactant 2

HCID 33557Sodium AzideHCID 20296129HCID 20296129, compound

Product 1

HCID 23329761HCID 23329761, compound

Reagents, catalysts & solvents 1

HCID 962WaterSolvent

Procedure

A solution of 3-chloromethyl-4-hydroxybenzeneacetic acid (0.1 mole) and sodium azide (0.1 mole) in 250 ml of water is stirred at room temperature for about 16 hours. Removal of the solvent gives the title compound combined with sodium chloride.

Workup

  1. customRemoval of the solvent

Sources & evidence

ORD record
ord-183b9e3354ac431c9ee007db0465f6d5
Source dataset
uspto-grants-1980_11
Patent number
US04236002

Reaction notes

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