Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Benzoyl chloride | HCID 7412 | — |
| Reactant | HCID 69130610 | HCID 69130610 | — |
| Solvent | Benzene | HCID 241 | — |
| Product | HCID 69130203 | HCID 69130203 | — |
Reaction Steps
A mixture of 2-(4-aminophenyl)-3-(3,5-dimethoxyphenyl)-N,N-dimethylacrylamide, 43, (0.49 g, 1.2 mmol) and benzoyl chloride (0.26 g, 1.8 mmol) in anhydrous benzene (18.0 mL) was heated at 90° C. for 2 h. Solvent was evaporated and crude product was purified by silica gel chromatography.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US07323496B2 |
|---|
| Source dataset | uspto-grants-2008_01 |
|---|
| ORD ID | ord-4e09059d6a39417098814cd748600709 |
|---|
| Source note | uspto-grants-2008_01 |
|---|
