HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzenesulfonamide → N-{3-[4-(1,2-diphenyl-but-1-enyl)-phenyl]-acryloyl}-benzenesulfonamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzenesulfonamide | HCID 7370 | — |
| Reactant | 3-[4-(Z)-(1,2-diphenylbut-1-enyl)phenyl]-acrylic acid | HCID 3036152 | — |
| Product | N-{3-[4-(1,2-diphenyl-but-1-enyl)-phenyl]-acryloyl}-benzenesulfonamide | HCID 69781534 | — |
Reaction Steps
Prepared from the coupling of 1a and benzene sulfonamide by the method described in Procedure 1, Method A. Yield (76%); 1H NMR (CDCl3) δ 8.41 (br. s, 1H), 8.08 (d, J=8.4 Hz, 2H), 7.65-7.07 (m, 16H), 6.86 (d, J=8.4 Hz, 2H), 6.23 (d, J=15.7 Hz, 1H), 2.46 (q, J=7.3 Hz, 2H), 0.92 (t, J=7.3 Hz, 3H); ESI m/z: 492 (M−H−, 100%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07323587B2 |
| Source dataset | uspto-grants-2008_01 |
| ORD ID | ord-680066e8482844778fa257c6e7f2ec27 |
| Source note | uspto-grants-2008_01 |