Methanesulfonamide → HCID 69780760, compound

HRID 2253447Notes

Reaction equation

HRID 2253447 reaction equation
[C:1]1([C:7]2[CH2:8][O:9][C:10]3[C:15]([C:16]=2[C:17]2[CH:22]=[CH:21][C:20]([CH:23]=[CH:24][C:25]([OH:27])=O)=[CH:19][CH:18]=2)=[CH:14][CH:13]=[CH:12][CH:11]=3)[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.[CH3:28][S:29]([NH2:32])(=[O:31])=[O:30]>>[C:1]1([C:7]2[CH2:8][O:9][C:10]3[C:15]([C:16]=2[C:17]2[CH:22]=[CH:21][C:20]([CH:23]=[CH:24][C:25]([NH:32][S:29]([CH3:28])(=[O:31])=[O:30])=[O:27])=[CH:19][CH:18]=2)=[CH:14][CH:13]=[CH:12][CH:11]=3)[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1

Participants

3

Reactant 2

HCID 72879MethanesulfonamideHCID 69317447HCID 69317447, compound

Product 1

HCID 69780760HCID 69780760, compound

Procedure

Prepared by coupling 3d and methylsulfonamide in accordance with Procedure 1, Method A described hereinabove. Yield (35%); ESI m/z: 430 (M−H−, 100%).

Workup

  1. customPrepared
  2. customYield (35%)

Sources & evidence

ORD record
ord-5da6ab6438c2419d9092908aa53b7514
Source dataset
uspto-grants-2008_01
Patent number
US07323587B2

Reaction notes

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