HuagongsheHuagongshe Chemistry Print Report · For research reference only
p-Cyanobenzenesulphonamide → 4-cyano-N-{3-[4-(1,2-diphenyl-but-1-enyl)-phenyl]-acryloyl}-benzenesulfonamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | p-Cyanobenzenesulphonamide | HCID 76566 | — |
| Reactant | 3-[4-(Z)-(1,2-diphenylbut-1-enyl)phenyl]-acrylic acid | HCID 3036152 | — |
| Product | 4-cyano-N-{3-[4-(1,2-diphenyl-but-1-enyl)-phenyl]-acryloyl}-benzenesulfonamide | HCID 69781487 | — |
Reaction Steps
Prepared by coupling 1a and 4-cyanobenzenesulfonamide in accordance with Procedure 1, Method B described hereinabove. Yield (21%); 1H NMR (d6-DMSO) δ 8.09-8.03 (m, 4H), 7.94 (d, J=8.0 Hz, 1H), 7.40-7.07 (m, 12H), 6.84 (d, J=8.0 Hz, 2H), 6.40 (d, J=15.7 Hz, 1H), 2.35 (q, J=7.4 Hz, 2H), 0.82 (t, J=7.4 Hz, 3H); APcI m/z: 519 (M+H+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07323587B2 |
| Source dataset | uspto-grants-2008_01 |
| ORD ID | ord-bb66fe0e37294aeea211039b5ee56e14 |
| Source note | uspto-grants-2008_01 |