HuagongsheHuagongshe Chemistry Print Report · For research reference only
P-Toluenesulfonamide → HCID 69320208, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | P-Toluenesulfonamide | HCID 6269 | — |
| Reactant | 3-[4-(Z)-(1,2-diphenylbut-1-enyl)phenyl]-acrylic acid | HCID 3036152 | — |
| Product | HCID 69320208 | HCID 69320208 | — |
Reaction Steps
Prepared by coupling 1a and p-toluenesulfonamide in accordance with Procedure 1, Method B described hereinabove. Yield (42%); 1H NMR (CD3OD) δ 7.87 (d, J=8.2 Hz, 2H), 7.37-7.08 (m, 15H), 6.87 (d, J=8.2 Hz, 2H), 6.32 (d, J=15.7 Hz, 1H), 2.44 (q, J=7.4 Hz, 2H), 2.40 (s, 3H), 0.89 (t, J=7.3 Hz, 3H); APcI m/z: 508 (M+H+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07323587B2 |
| Source dataset | uspto-grants-2008_01 |
| ORD ID | ord-d8e08d4c6c234d60aefde12c6d9a2041 |
| Source note | uspto-grants-2008_01 |