HuagongsheHuagongshe Chemistry Print Report · For research reference only
Chloroacetonitrile → HCID 19745800, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Chloroacetonitrile | HCID 7856 | — |
| Reactant | HCID 19745798 | HCID 19745798 | — |
| Product | HCID 19745800 | HCID 19745800 | — |
Reaction Steps
Analogously to the procedure described in Example 81, by alkylating 3-(3,4-dihydro-7-fluoro-3-oxo-2H-1,4-benzoxazin-6-yl)-6-methyl-2,4(1H,3H)-pyrimidinedione (see Example 21) with chloroacetonitrile there is obtained 3-(2-cyanomethyl-3,4-dihydro-7-fluoro-3-oxo-2H-1,4-benzoxazin-6-yl)-6-methyl-2,4(1H,3H)-pyrimidinedione, m.p.>230° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05232898 |
| Source dataset | uspto-grants-1993_08 |
| ORD ID | ord-5d3d5af04182400784e0d18807c595b3 |
| Source note | uspto-grants-1993_08 |