HuagongsheHuagongshe Chemistry Print Report · For research reference only
Bromotriphenylmethane → 4,4-Dimethyl-1-iodo-3-triphenylmethoxy-trans-1-octene
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Bromotriphenylmethane | HCID 11692 | — |
| Reactant | 4,4-Dimethyl-1-iodo-trans-1-octen-3-ol | HCID 20465723 | — |
| Product | 4,4-Dimethyl-1-iodo-3-triphenylmethoxy-trans-1-octene | HCID 20465743 | — |
Reaction Steps
Treatment of 11.2 g. (0.396 mole) of 4,4-dimethyl-1-iodo-trans-1-octen-3-ol (Example 151) with 12.8 g. of triphenylmethyl bromide in 50 ml. of pyridine and purification on Florisil®, all as described in Example 127 gives the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04236027 |
| Source dataset | uspto-grants-1980_11 |
| ORD ID | ord-3894d4f21d2f4536b396d984ae3013c8 |
| Source note | uspto-grants-1980_11 |