HuagongsheHuagongshe Chemistry Print Report · For research reference only
Isopropanol → HCID 85937510, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Isopropanol | HCID 3776 | — |
| Reactant | Methanesulfonic Acid | HCID 6395 | — |
| Reactant | 3-Phenoxypyridine | HCID 200510 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | HCID 85937510 | HCID 85937510 | — |
Reaction Steps
A solution of 18 g. of 3-phenoxypyridine in 100 ml. of 2-propanol is treated with 9.6 g. of methanesulfonic acid with stirring. The solution is diluted with ether and the crystalline precipitate of 3-phenoxypyridine methanesulfonate is collected, washed with ether and dried at reduced pressure; m.p. 121°-123° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05232934 |
| Source dataset | uspto-grants-1993_08 |
| ORD ID | ord-d3ee9fd6226d4798a749a644bc0783a8 |
| Source note | uspto-grants-1993_08 |