HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Toluenesulfonyl chloride → 3-[2-(4-Methylbenzenesulfonyloxy)ethyl]-6,7,8,9-tetrahydro-2H-pyrido[1,2-a]-1,3,5-triazine-2,4(3H)-dione
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Toluenesulfonyl chloride | HCID 7397 | — |
| Reactant | 3-(2-hydroxyethyl)-6,7,8,9-tetrahydro-2H-pyrido[1,2-a]-1,3,5-triazine-2,4(3H)-dione | HCID 19746034 | — |
| Product | 3-[2-(4-Methylbenzenesulfonyloxy)ethyl]-6,7,8,9-tetrahydro-2H-pyrido[1,2-a]-1,3,5-triazine-2,4(3H)-dione | HCID 19745994 | — |
Reaction Steps
The entitled compound was prepared as a yellowish solid from 3-(2-hydroxyethyl)-6,7,8,9-tetrahydro-2H-pyrido[1,2-a]-1,3,5-triazine-2,4(3H)-dione prepared in Reference Example 27 and 4-methylbenzenesulfonyl chloride in the manner described in Reference Example 33.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05232924 |
| Source dataset | uspto-grants-1993_08 |
| ORD ID | ord-fa954e74849141b8a26ccbb1478eb1ca |
| Source note | uspto-grants-1993_08 |