HuagongsheHuagongshe Chemistry Print Report · For research reference only
Bromotriphenylmethane → 4,4-Dimethyl-3-triphenylmethoxy-1-octyne
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Bromotriphenylmethane | HCID 11692 | — |
| Reactant | 4,4-Dimethyl-1-octyn-3-ol | HCID 14516369 | — |
| Product | 4,4-Dimethyl-3-triphenylmethoxy-1-octyne | HCID 23329946 | — |
Reaction Steps
Treatment of 23.1 g. (0.150 mole) of 4,4-dimethyl-1-octyn-3-ol (Example 149) with 56.5 g. of triphenylmethyl bromide in 150 ml. of pyridine and purification of Florisil®, all as described in Example 127 gives the title compound, m.p. 75°-77° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04236027 |
| Source dataset | uspto-grants-1980_11 |
| ORD ID | ord-40ff8d2c09134fdeb184ee23a7ffff55 |
| Source note | uspto-grants-1980_11 |