HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanol → N,N,N-Triethyl-3-(trimethoxysilyl)propan-1-aminium chloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanol | HCID 887 | — |
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | 3-(Trimethoxysilyl)propyl chloride | HCID 62449 | — |
| Solvent | Isopropanol | HCID 3776 | — |
| Product | N,N,N-Triethyl-3-(trimethoxysilyl)propan-1-aminium chloride | HCID 14552288 | — |
Reaction Steps
A mixture of 60.0 grams of methanol, 60.0 grams of chloropropyltrimethoxysilane and 19.53 grams of triethylamine was prepared. The mixture was heated and allowed to reflux for 96 hours. A pinkish tint was observed. The mixture was vacuum stripped at 80° C. and 29 inches of Hg, for one hour. The mixture became brown in color. Upon cooling, solidified to form a crystal salt. To 8.0 grams of the product was added 2.0 grams of isopropanol wherein the salt dissolved.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05232964 |
| Source dataset | uspto-grants-1993_08 |
| ORD ID | ord-cfdc8ac28a134c69b9215510a7035d72 |
| Source note | uspto-grants-1993_08 |